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Interdependent Dynamic Nitroaldol and Boronic Ester Reactions for Complex Dynamers of Different Topologies
KTH Royal Instute of Technology, Sweden.ORCID iD: 0000-0001-8020-0579
Univ Massachusetts Lowell, USA.ORCID iD: 0000-0002-3707-9504
Univ Massachusetts Lowell, USA.ORCID iD: 0000-0001-8370-246X
KTH Royal Instute of Technology, Sweden.
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2024 (English)In: Chemistry - A European Journal, ISSN 0947-6539, E-ISSN 1521-3765, Vol. 30, no 63, article id e202402409Article in journal (Refereed) Published
Abstract [en]

Complex dynamic systems displaying interdependency between nitroaldol and boronic ester reactions have been demonstrated. Nitroalkane-1,3-diols, generated by the nitroaldol reaction, were susceptible to ester formation with different boronic acids in aprotic solvents, whereas hydrolysis of the esters occurred in the presence of water. The boronic ester formation led to significant stabilization of the nitroaldol adducts under basic conditions. The use of bifunctional building blocks was furthermore established, allowing for main chain nitroaldol-boronate dynamers as well as complex network dynamers with distinct topologies. The shape and rigidity of the resulting dynamers showed an apparent dependency on the configuration of the boronic acids.

Place, publisher, year, edition, pages
John Wiley & Sons, 2024. Vol. 30, no 63, article id e202402409
Keywords [en]
Dynamic covalent, Nitroaldol, Boronate, Dynamer, Topology
National Category
Organic Chemistry
Research subject
Chemistry, Organic Chemistry
Identifiers
URN: urn:nbn:se:lnu:diva-133462DOI: 10.1002/chem.202402409ISI: 001339776900001PubMedID: 39183180Scopus ID: 2-s2.0-85207152228OAI: oai:DiVA.org:lnu-133462DiVA, id: diva2:1914511
Available from: 2024-11-19 Created: 2024-11-19 Last updated: 2025-01-14Bibliographically approved

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Ramström, Olof

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Karalius, AntanasQi, YunchuanAyinla, MubarakRamström, Olof
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