lnu.sePublications
Change search
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf
Preparation, characterization and application of a stationary chromatographic phase from a new (+)-tartaric acid derivative
Linnaeus University, Faculty of Science and Engineering, School of Natural Sciences. (BBCL)ORCID iD: 0000-0002-0407-6542
Show others and affiliations
2010 (English)In: Tetrahedron Letters, ISSN 0040-4039, E-ISSN 1359-8562, Vol. 51, no 17, p. 2258-2261Article in journal (Refereed) Published
Abstract [en]

The preparation, characterization and application of a new stationary phase derived from 1,4-cyclohexanedione and diethyl (+)-tartrate are described. A suitable TADDOL for immobilization has been synthesized and grafted to a gamma-mercaptopropylsilylated silica gel. The resulting modified stationary phase has been characterized and its ability to separate enantiomers has been studied. While the free TADDOL in solution was able to resolve a range of enantiomers, the resolving properties were lost on immobilization. Solid state C-13 CPMAS NMR of the new stationary phase was used to explain the lack of stereoselective recognition. (C) 2010 Elsevier Ltd. All rights reserved.

Place, publisher, year, edition, pages
2010. Vol. 51, no 17, p. 2258-2261
National Category
Analytical Chemistry
Research subject
Natural Science, Ecological chemistry
Identifiers
URN: urn:nbn:se:lnu:diva-12406DOI: 10.1016/j.tetlet.2010.02.101ISI: 000276588100013Scopus ID: 2-s2.0-77949774041OAI: oai:DiVA.org:lnu-12406DiVA, id: diva2:422394
Available from: 2011-06-13 Created: 2011-06-13 Last updated: 2017-12-11Bibliographically approved

Open Access in DiVA

No full text in DiVA

Other links

Publisher's full textScopus

Authority records

Nicholls, Ian A.Unelius, C. Rikard

Search in DiVA

By author/editor
Nicholls, Ian A.Unelius, C. Rikard
By organisation
School of Natural Sciences
In the same journal
Tetrahedron Letters
Analytical Chemistry

Search outside of DiVA

GoogleGoogle Scholar

doi
urn-nbn

Altmetric score

doi
urn-nbn
Total: 162 hits
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf