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Preparation, characterization and application of a stationary chromatographic phase from a new (+)-tartaric acid derivative
Linnaeus University, Faculty of Science and Engineering, School of Natural Sciences. (BBCL)ORCID iD: 0000-0002-0407-6542
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2010 (English)In: Tetrahedron Letters, ISSN 0040-4039, E-ISSN 1359-8562, Vol. 51, no 17, p. 2258-2261Article in journal (Refereed) Published
Abstract [en]

The preparation, characterization and application of a new stationary phase derived from 1,4-cyclohexanedione and diethyl (+)-tartrate are described. A suitable TADDOL for immobilization has been synthesized and grafted to a gamma-mercaptopropylsilylated silica gel. The resulting modified stationary phase has been characterized and its ability to separate enantiomers has been studied. While the free TADDOL in solution was able to resolve a range of enantiomers, the resolving properties were lost on immobilization. Solid state C-13 CPMAS NMR of the new stationary phase was used to explain the lack of stereoselective recognition. (C) 2010 Elsevier Ltd. All rights reserved.

Place, publisher, year, edition, pages
2010. Vol. 51, no 17, p. 2258-2261
National Category
Analytical Chemistry
Research subject
Natural Science, Ecological chemistry
Identifiers
URN: urn:nbn:se:lnu:diva-12406DOI: 10.1016/j.tetlet.2010.02.101ISI: 000276588100013Scopus ID: 2-s2.0-77949774041OAI: oai:DiVA.org:lnu-12406DiVA, id: diva2:422394
Available from: 2011-06-13 Created: 2011-06-13 Last updated: 2017-12-11Bibliographically approved

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Nicholls, Ian A.Unelius, C. Rikard

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