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  • 1.
    Dagbro, Ola
    Luleå University of Technology, Sweden.
    Studies on Industrial-Scale Thermal Modification of Wood2016Doktoravhandling, med artikler (Annet vitenskapelig)
    Abstract [en]

    Wood as a raw material is useful for many purposes even though some properties are less than optimal, for example, dimensional stability and durability. These characteristics can however be improved by different treatment methods. Environmental awareness has led to an increased demand for environmentally friendly processes like thermal modification that does not add any chemicals to the wood in contrast to, for example, CCA-impregnated wood.This thesis mainly focuses on thermally modified wood from species such as pine, spruce and birch. The thesis present studies of physical attributes such as color, and chemical analysis of water-soluble compounds and degradation products. Treatment intensity is compared between two different industrial processes referred as Thermowood and WTT, which use respectively superheated steam and pressurized steam as heating media.Thermal modification processes darken the color of wood throughout its cross-section. The formation of darker color is related to a degradation processes that takes place during thermal modification. During thermal modification wood is exposed to temperatures between 160 - 220°C, and the temperature causes physical and chemical transformations that change some of the wood properties. Dimensional stability and durability are typically improved, but mechanical strength properties are usually negatively affected by the treatment.The studied wood species were Scots pine (Pinus sylvestris L.), Norway spruce (Picea abies L.) and Birch (Betula pendula L.). Treatments using pressurized steam were carried out under temperatures of 160°C, 170°C and 180°C, and treatments using superheated steam at normal air pressure were carried out at temperatures of 190°C and 212°C. Results showed that similar L* (lightness) can be reached at lower temperatures using pressurized steam compared to superheated steam. The residual moisture content after completed thermal modification was approximately 10% higher in wood treated with the pressurized steam process. It was found that despite an approximately 25°C lower treatment temperature, birch modified in pressurized steam was more acidic compared to birch modified in superheated steam. This will likely have further consequences, requiring more research concerning surface treatment and fixation.The thesis also includes the development of an industrial-quality control procedure based on nondestructive color measurements verified in industrial environment. Treatment intensity in industry is today certified by inspection of documented process schedule and measuring the temperature and time of the process. Quality control in this context refers to the measurement of wood color as an indirect measure of treatment intensity. The color in our study was measured using L*C*H color space. The study shows that it is possible for quality control purposes to measure the color of thermally modified wood from the surfaces of planed boards instead of sawdust or board cross sections that have been used in other studies.The thesis has a final section about academia-industry collaboration that describes how trust building was established through a fruitful relationship involving academia and regional wood products industry in northern Sweden. The study presents an example of a successful research and development alliance between university and a group of small- and medium-sized enterprises (SMEs). This alliance has been a great example on international collaboration involving researchers originating from Finland, China, Bangladesh, Spain, Russia and Sweden. Through an in-depth multi-year study of how the research cooperation developed, the paper describes how the involved companies successfully entered into a new segment of the market.

  • 2.
    Dagbro, Ola
    et al.
    Linnéuniversitetet, Universitetsförvaltningen. Linnéuniversitetet.
    Torniainen, Petteri
    Department of Forest Products, Swedish University of Agricultural Sciences, Uppsala.
    Karlsson, Olov
    Luleå tekniska universitet, Träteknik.
    Morén, Tom
    Luleå tekniska universitet, Träteknik.
    Colour responses from wood, thermally modified in superheated steam and pressurized steam atmospheres2010Inngår i: Wood Material Science & Engineering, ISSN 1748-0272, E-ISSN 1748-0280, Vol. 5, nr 3, s. 211-219Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    In this study, two different methods were used to produce thermally modified wood. One was carried out in a typical kiln drying chamber using superheated steam (SS) and the other used pressurized steam in an autoclave cylinder (PS). Overall, both processes followed the same principles and the wood was not treated with any chemicals. Two wood species were studied, Scots pine (Pinus sylvestris) and Norway spruce (Picea abies). Treatments in the autoclave were carried out under pressure using temperatures of 160°C, 170°C and 180°C. Temperatures of 190°C and 212°C were used in treatments in the chamber at normal air pressure. The colour was measured using L*C*H colour space. Results for both species showed that similar L* (lightness) can be reached at lower (20-308C) temperatures using PS compared with SS treatment. The hue angle of PS-treated wood was smaller than that of SS-treated wood. No significant difference in C* (chroma) was detected. The difference in E value between PS- and SS-treated wood was smaller for Norway spruce than for Scots pine. The residual moisture content was about 10% higher in wood treated by the PS process compared with the SS process

  • 3.
    Dagbro, Ola
    et al.
    Linnéuniversitetet, Universitetsförvaltningen. Linnéuniversitetet.
    Torniainen, Petteri
    Luleå tekniska universitet, Träteknik.
    Morén, Tom
    Luleå tekniska universitet, Träteknik.
    Thermal modification of birch using saturated and superheated steam2011Inngår i: Proceedings of the 7th meeting of the Nordic-Baltic Network in Wood Material Science and Engineering (WSE): October 27-28, 2011, Oslo, Norway / [ed] Erik Larnøy; Gry Alfredsen, Ås: Norsk institutt for skog og landskap , 2011, s. 43-48Konferansepaper (Fagfellevurdert)
    Abstract [en]

    During the thermal modification, wood is normally exposed to temperatures between 160 - 220°C. As a result physical and chemical changes are taking place and some of the wood properties are changed. Dimensional stability and weather resistance are improved. On the other hand the mechanical strength properties are usually negatively affected by the treatment. The visual appearance is also changed. There were two different types of thermal modification processes used in this study. One of them was using saturated steam and the other one superheated steam. Treatment temperature was 160°C in saturated steam process and 185°C in superheated steam. The wood specie used in this study was Silver birch (Betula pendula). In the chemistry part the acid content was investigated. Despite the 25°C lower treatment temperature, birch modified in saturated steam was more acidic compared to birch modified in superheated steam. Some differences in equilibrium moisture content (EMC) and dimensional stability were found mainly in the environment T=20°C and RH=85%. The colour of birch treated in saturated steam at 160°C was darker than the colour of birch treated in superheated steam at temperature 185°C.

  • 4.
    Dorn, Michael
    et al.
    Linnéuniversitetet, Fakulteten för teknik (FTK), Institutionen för byggteknik (BY).
    Tuvendal, Helena
    Södra skogsägarna.
    Henrik, Oxfall
    Swerea.
    Serrano, Erik
    Lunds Tekniska Högskola.
    FBBB 4.3 Biobaserade skivmaterial: Experimentella undersökningar2018Rapport (Annet vitenskapelig)
    Abstract [sv]

    Rapporten är del av projektet Framtidens Byggande och Boende (FBBB), delprojekt 4.3 "Biobaserade skivmaterial". I denna rapport presenteras resultatet av de mekaniska drag- och böjprov såsom DTMA analys. Materialet ”Durapulp”, som tillverkas av Södra, är referensmaterialet i delprojektet. Provkroppar av Durapulp producerades med olika tillverkningsmetoder för att se skillnader i beteenden. Referensmaterialen är trä-baserade skivmaterial som anses vanligt förekommande i byggskeendet.

  • 5.
    Hosseinpourpia, Reza
    et al.
    Linnéuniversitetet, Fakulteten för teknik (FTK), Institutionen för skog och träteknik (SOT).
    Adamopoulos, Stergios
    Linnéuniversitetet, Fakulteten för teknik (FTK), Institutionen för skog och träteknik (SOT).
    Parsland, Charlotte
    Linnéuniversitetet, Fakulteten för teknik (FTK), Institutionen för byggd miljö och energiteknik (BET).
    Utilization of different tall oils for improving the water resistance of cellulosic fibers2019Inngår i: Journal of Applied Polymer Science, ISSN 0021-8995, E-ISSN 1097-4628, Vol. 136, nr 13, artikkel-id 47303Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    This study was conducted to assess the effect of the pulping by-products crude tall oil (CTO), distilled tall oil (DTO), andtall oil fatty acid (TOFA) on dynamic water vapor sorption behavior, interfiber strength, and thermal stability of cellulosic paper-sheets.The results were compared against those obtained in cellulose papers treated with the conventional petroleum-derived hydrophobicagent hydrowax and in untreated ones. The tall oil treatments caused strong reduction in equilibrium moisture content of the paper-sheets during adsorption and desorption runs. The same trend was noticed for the hydrowax-treated papers, however, it was lesspronounced than the CTO-treated and DTO-treated samples in the relative humidity range of 75–95%. The sorption hysteresis was con-siderably decreased after the treatments. The ultimate dry-tensile strengths of the paper-sheets were significantly reduced by TOFA andhydrowax treatments, while CTO and DTO showed comparable strength as that of untreated control. The ultimate wet-strengths of thepaper-sheets were improved after the treatments. The thermal stability of the specimens was improved by the tall oil treatments, and thehydrowax-treated samples illustrated lower degradation temperature than the untreated control. The results are promising for the use oftall oils as alternative hydrophobic agents of cellulosicfiber-based products, such as wood panels and paper packaging.

  • 6.
    Karlsson, Olov
    et al.
    Luleå tekniska universitet, Träteknik.
    Dagbro, Ola
    Luleå tekniska universitet, Träteknik.
    Granlund, Kurt
    Luleå tekniska universitet, Institutionen för teknikvetenskap och matematik.
    Soluble degradation products in thermally modified wood2014Inngår i: Final Cost Action FP0904 Conference: “Recent Advances in the Field of TH and THM Wood Treatment” : May 19-21, 2014, Skellefteå, Sweden : book of abstracts / [ed] Mojgan Vaziri; Dick Sandberg, Skellefteå: Luleå tekniska universitet , 2014, s. 16-17Konferansepaper (Fagfellevurdert)
  • 7.
    Karlsson, Olov
    et al.
    Luleå tekniska universitet, Träteknik.
    Torniainen, Petteri
    Luleå tekniska universitet, Träteknik.
    Dagbro, Ola
    Luleå tekniska universitet, Träteknik.
    Granlund, Kurt
    Luleå tekniska universitet, Institutionen för teknikvetenskap och matematik.
    Morén, Tom
    Luleå tekniska universitet, Träteknik.
    Presence of water-soluble compounds in thermally modified wood: carbohydrates and furfurals2012Inngår i: BioResources, ISSN 1930-2126, E-ISSN 1930-2126, Vol. 7, nr 3, s. 3679-3689Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    With thermal modification, changes in properties of wood, such as the presence of VOC and water-soluble carbohydrates, may occur. Thermal modifications under saturated steam conditions (160°C or 170°C) and superheated steam conditions (170, 185, and 212°C) were investigated by analysing the presence of water-soluble 5-(hydroxymethyl)furfural (HMF), furfural, and carbohydrates in heat-treated wood. The influence of thermal modifications on Scots pine, Norway spruce, and silver birch was also studied. Furfurals were analysed using HPLC at 280 nm, while monosaccharides and water-soluble carbohydrates were determined by GC-FID as their acetylated alditiols and, after methanolysis, as their trimethylsilylated methyl-glycosides, respectively. The amount of furfurals was larger in boards thermally modified under saturated steam conditions than those treated under superheated steam conditions. Generally, more of HMF than furfural was found in the thermally modified boards. In process water, in which saturated steam conditions had been used, furfural and only traces of HMF were found. Higher content of water-soluble carbohydrates was found in boards treated in saturated steam rather than in superheated steam. After modification in saturated steam, substantial parts of the water-soluble carbohydrates were due to monosaccharides, but only traces of monosaccharides were found in boards treated under superheated steam conditions.

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